PREPARATION OF N-PROTECTED α-AMINO ALCOHOLS BY ACETOXYBOROHYDRIDE REDUCTION OF N-PROTECTED α-AMINO ACID ESTERS
N-Protected α-amino alcohols were prepared by reduction of N-protected α-amino acid esters by sodium acetoxyborohydride in dioxane at elevated temperature.The reductions proceed with excellent yields and without racemisation.Reduction of the carbamate protecting groups was not observed.
Soucek, Milan,Urban, Jan,Saman, David
p. 761 - 765
(2007/10/02)
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