Journal of Sulfur Chemistry p. 515 - 528 (2016)
Update date:2022-08-05
Topics:
Truong, Binh Nhat
Le, Luong Huu
Chau, Duy-Khiem Nguyen
Duus, Fritz
Luu, Thi?Xuan?Thi
The sulfonylation reaction of various aliphatic, alicyclic, aromatic, and hetero-aromatic amines with p-acetamidobenzenesulfonyl chloride has been investigated using different types of base catalysis under varied reaction conditions. Mg–Al hydrotalcite, characterizable as an inexpensive, reusable, and green solid catalyst, was found to be the most efficient catalyst, when the reaction is carried out in a minimum volume of solvent (acetone). The reaction was found to be accelerated drastically with the support of ultrasound irradiation, affording the sulfonamides in yields better or equivalent to those obtained under the longer lasting conventional stirring conditions.
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