Bulletin of the Chemical Society of Japan p. 1754 - 1758 (1993)
Update date:2022-08-17
Topics:
Yoshino, Norio
Yamamoto, Yasushi
Hamano, Katsumi
Kawase, Tokuzo
Four silane coupling agents, (1H,1H,2H,2H-polyfluoroalkyl)trimethoxysilanes ((1H,1H,2H,2H-henicosafluorododecyl)trimethoxysilane, C10F21C2H4Si(OCH3)3, (1H,1H,2H,2H-heptadecafluorodecyl)trimethoxysilane, C58F17C2H4Si(OCH3)3, (1H,1H,2H,2H-tridecafluorooctyl)trimethoxysilane, C6F13C2H4Si(OCH3)3, and (1H,1H,2H,2H-nonafluorohexyl)trimethoxysilane, C4F9C2H4Si(OCH3)3), were prepared by the hydrosilylation of trichlorosilane with the corresponding 1H,1H,2H,-polyfluoro-1-alkene in the presence of hydrogen hexachloroplatinate-(IV), followed by reaction with sodium methoxide.The surface modification of glass plate was attempted using these products.From measurements of the contact angles θ (deg) of water and oleic acid against a modified glass plate surface, the coupling agents were found to have high modification ability.The modification produced a glass surface with high oxidation resistance.
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