2,2'-(Methylazanediyl)dipropanenitrile

Base Information

• Chemical Name: 2,2'-(Methylazanediyl)dipropanenitrile
• CAS No.: 57768-53-3
• Molecular Formula: C7H11N3
• Molecular Weight: 137.184
• DSSTox Substance ID: DTXSID30534005
• Mol file: 57768-53-3.mol

Synonyms:2,2'-(Methylazanediyl)dipropanenitrile;57768-53-3;SCHEMBL9343649;DTXSID30534005;AKOS011163224

Chemical Property of 2,2'-(Methylazanediyl)dipropanenitrile

Chemical Property:

• XLogP3: 0.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 137.095297364
• Heavy Atom Count: 10
• Complexity: 169

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C#N)N(C)C(C)C#N

Technology Process of 2,2'-(Methylazanediyl)dipropanenitrile

There total 7 articles about 2,2'-(Methylazanediyl)dipropanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

potassium carbonate (584-08-7) → methylaminopropionitrile (16752-54-8) + α-methylaminodipropionitrile (57768-53-3) + carbamate de l' α-N-methylaminopropionitrile

Guidance literature:

With potassium hydroxide; In water-d2; at 29 ℃; Yields of byproduct given; pH: 9;

DOI:10.1016/0040-4020(80)80137-2

Reference yield:

methylaminopropionitrile (16752-54-8) + acetaldehyde (75-07-0,9002-91-9) → α-methylaminodipropionitrile (57768-53-3) + 2-hydroxy-propionitrile (78-97-7)

Guidance literature:

With hydrogen cyanide; carbon dioxide; methylamine; In water; at 50 ℃; Product distribution; pH = 8.9, other reagents;

Reference yield:

methylaminopropionitrile (16752-54-8) → 1,5-dimethylimidazolidine-2,4-dione (17374-27-5) + α-methylaminodipropionitrile (57768-53-3) + carbamate de l' α-N-methylaminopropionitrile + 2-hydroxy-propionitrile (78-97-7)

Guidance literature:

With sodium carbonate; at 50 ℃; Product distribution;

DOI:10.1016/0040-4020(80)80137-2

upstream raw materials:

1,5-dimethylimidazolidine-2,4-dione

methylaminopropionitrile

sodium carbonate

potassium carbonate

Downstream raw materials:

1,5-dimethylimidazolidine-2,4-dione

methylaminopropionitrile

2-hydroxy-propionitrile

Refernces

• 1、 Rousset, A.,Lasperas, M.,Taillades, J.,Commeyras, A.. "Systemes de Strecker et apparentes XV. Comportement d'α-alcoylaminonitriles en presence de CS2 et de CO2". . p. 209 - 216. Retrieved 2007/10/02.