Benzenesulfonothioic acid, 3-methoxy-, ammonium salt

Base Information

• Chemical Name: Benzenesulfonothioic acid, 3-methoxy-, ammonium salt
• CAS No.: 77853-08-8
• Molecular Formula: C7H8O3S2.H3N
• Molecular Weight: 221.301
• Mol file: 77853-08-8.mol

Synonyms:

Chemical Property of Benzenesulfonothioic acid, 3-methoxy-, ammonium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenesulfonothioic acid, 3-methoxy-, ammonium salt

There total 1 articles about Benzenesulfonothioic acid, 3-methoxy-, ammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

1-methoxy-3-(4-nitrobenzenesulfonyl)benzene (77863-75-3) → di(p-nitrophenyl) disulfide (100-32-3) + 3-Methoxy-benzenethiosulfonic acid; compound with ammonia (77853-08-8) + 4-nitro-aniline (100-01-6,104810-17-5)

Guidance literature:

With sulfur; ammonia; at 100 ℃; for 2h; titanium autoclave;

DOI:10.1055/s-1981-29327

upstream raw materials:

1-methoxy-3-(4-nitrobenzenesulfonyl)benzene

Refernces