N(1)-methyl-2-bromo-lysergic acid diethylamide

Base Information

• Chemical Name: N(1)-methyl-2-bromo-lysergic acid diethylamide
• CAS No.: 50484-98-5
• Molecular Formula: C₂₁H₂₆BrN₃O
• Molecular Weight: 416.361
• Mol file: 50484-98-5.mol

Synonyms:Lysergamide,2-bromo-N,N-diethyl-1-methyl- (6CI,7CI); Indolo[4,3-fg]quinoline,ergoline-8-carboxamide deriv.; 1-Methyl-2-bromo-LSD

Chemical Property of N(1)-methyl-2-bromo-lysergic acid diethylamide

Chemical Property:

• Vapor Pressure: 1.69E-13mmHg at 25°C
• Boiling Point: 581.2°C at 760 mmHg
• Flash Point: 305.3°C
• PSA: 28.48000
• Density: 1.41g/cm³
• LogP: 3.61680

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N(1)-methyl-2-bromo-lysergic acid diethylamide

There total 2 articles about N(1)-methyl-2-bromo-lysergic acid diethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-lysergide (478-84-2) → 2-bromo-1,6-dimethyl-9,10-didehydro-ergoline-8β-carboxylic acid diethylamide (50484-98-5)

Guidance literature:

With ammonia; potassium amide; und anschliessend mit CH₃I in Aether;

DOI:10.1002/hlca.19570400716

Reference yield:

lysergide (50-37-3) → 2-bromo-1,6-dimethyl-9,10-didehydro-ergoline-8β-carboxylic acid diethylamide (50484-98-5)

Guidance literature:

Multi-step reaction with 2 steps

1: /BRN= 42790/

2: KNH₂; liquid NH₃ / und anschliessend mit CH₃I in Aether

With ammonia; potassium amide;

DOI:10.1002/hlca.19570400716

upstream raw materials:

2-bromo-lysergide

lysergide