Diethanolamine hydrochloride

Base Information

• Chemical Name: Diethanolamine hydrochloride
• CAS No.: 14426-21-2
• Molecular Formula: C4H11 N O2 . Cl H
• Molecular Weight: 141.598
• European Community (EC) Number: 238-396-4
• UNII: OI45OUW092
• DSSTox Substance ID: DTXSID10884752
• Wikidata: Q27285664
• Mol file: 14426-21-2.mol

Synonyms:diethanolamine;diethanolamine acetate;diethanolamine bisulfate;diethanolamine fumarate;diethanolamine hydrochloride;diethanolamine maleate;diethanolamine maleate (1:1);diethanolamine phosphate;diethanolamine sulfate (1:1);diethanolamine sulfate (2:1);diethanolamine sulfite;diethanolamine sulfite (1:1);diethanolammonium sulfate

Chemical Property of Diethanolamine hydrochloride

Chemical Property:

• Vapor Pressure: 0.00104mmHg at 25°C
• Melting Point: -26 °C
• Refractive Index: n20/D 1.517(lit.)
• Boiling Point: 239.4°Cat760mmHg
• Flash Point: 90.5°C
• PSA: 52.49000
• Density: 0.996g/cm³
• LogP: -0.24650
• Storage Temp.: Inert atmosphere,Room Temperature
• Water Solubility.: Soluble in water
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 141.0556563
• Heavy Atom Count: 8
• Complexity: 28.9

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,2''-Azanediyldiethanolhydrochloride ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C(CO)NCCO.Cl
• Uses: Diethanolamine hydrochloride was used in the synthesis of:N-monophenylpiperazinediethanolammonium chloride, required for the preparation of diethanolammonium-tetrachloridopalladate(II) complex

Technology Process of Diethanolamine hydrochloride

There total 1 articles about Diethanolamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-iminobis[ethanol] (111-42-2) → diethanolamine hydrochloride (14426-21-2)

Guidance literature:

With hydrogenchloride; In dichloromethane; water; at 20 ℃;

DOI:10.1016/j.bioorg.2009.07.003

Reference yield: 92.0%

diethanolamine hydrochloride (14426-21-2) → nitro-bis-(2-nitryloxy-ethyl)-amine (4185-47-1)

Guidance literature:

With nitric acid; acetic anhydride; at 5 - 40 ℃; for 5.55556h; Concentration; Temperature; Thermodynamic data;

DOI:10.1021/acs.oprd.9b00300

Reference yield: 60.0%

aniline hydrochloride (142-04-1,36663-09-9) + diethanolamine hydrochloride (14426-21-2) → 4-phenyl-1-piperazine (92-54-6)

Guidance literature:

at 220 - 240 ℃;

DOI:10.1007/s00044-007-9007-x

upstream raw materials:

2,2'-iminobis[ethanol]

Downstream raw materials:

4-phenyl-1-piperazine

bis(2-phenylaminoethyl)amine

morpholine

piperazine

Refernces

• 1、 Petrovi?, Zorica D.,Simijonovi??, Duica,Petrovi?, Vladimir P.,Markovi?, Svetlana. "Diethanolamine and N,N-diethylethanolamine ionic liquids as precatalyst-precursors and reaction media in green Heck reaction protocol". experimental part. p. 45 - 50. Retrieved 2010/11/16.