DINITROSODIMETHYLPROPANEDIAMINE

Base Information

• Chemical Name: DINITROSODIMETHYLPROPANEDIAMINE
• CAS No.: 6972-76-5
• Molecular Formula: C5H12 N4 O2
• Molecular Weight: 160.176
• Mol file: 6972-76-5.mol

Synonyms:1,3-Propanediamine,N,N'-dimethyl-N,N'-dinitroso- (7CI,8CI,9CI); NSC 62580

Chemical Property of DINITROSODIMETHYLPROPANEDIAMINE

Chemical Property:

• Refractive Index: 1.7900 (estimate)
• Boiling Point: 286.07°C (rough estimate)
• Flash Point: 175.4oC
• PSA: 65.34000
• Density: 1.2833 (rough estimate)
• LogP: 0.60290

Purity/Quality:

99% ^*data from raw suppliers

DINITROSODIMETHYLPROPANEDIAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DINITROSODIMETHYLPROPANEDIAMINE

There total 3 articles about DINITROSODIMETHYLPROPANEDIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

N,N,N'N'-tetramethyl-1,3-propanediamine (110-95-2) → N-Nitrosodimethylamine (62-75-9) + 1,3-Bis-methylnitrosamino-propan (6972-76-5)

Guidance literature:

With dinitrogen tetraoxide; In tetrachloromethane; at 0 - 45 ℃; for 15h;

Reference yield:

N,N'-Dimethyl-propane-1,3-diamine; hydrochloride → 1,3-Bis-methylnitrosamino-propan (6972-76-5)

Guidance literature:

With sodium nitrite;

DOI:10.1039/jr9630000846

Reference yield:

1,3-bis(methylamino)propane (111-33-1) → 1,3-Bis-methylnitrosamino-propan (6972-76-5)

Guidance literature:

With hydrogenchloride; sodium nitrite;

upstream raw materials:

1,3-bis(methylamino)propane

N,N,N'N'-tetramethyl-1,3-propanediamine

Downstream raw materials:

1,3-Di<2-(p-nitrobenzyliden)-1-methylhydrazino>propan

Refernces