propyl hydrogen sulfate

Base Information

• Chemical Name: propyl hydrogen sulfate
• CAS No.: 13425-84-8
• Molecular Formula: C3H8O4S
• Molecular Weight: 140.16
• Mol file: 13425-84-8.mol

Synonyms:

Chemical Property of propyl hydrogen sulfate

Chemical Property:

• Density: 1.361g/cm³

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of propyl hydrogen sulfate

There total 2 articles about propyl hydrogen sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

propan-1-ol (71-23-8) + diammonium salt of phenyl phosphatosulfate (32599-82-9) → sulfuric acid monopropyl ester (13425-84-8) + phosphoric acid monophenyl ester (701-64-4) + phenyl n-propyl hydrogen phosphate (17123-02-3)

Guidance literature:

With N-ethylmorpholine;; magnesium(II) perchlorate; at 55 ℃; Rate constant;

DOI:10.1246/bcsj.66.2931

Reference yield:

propan-1-ol (71-23-8) → sulfuric acid monopropyl ester (13425-84-8) + propyl bromide (106-94-5)

Guidance literature:

With sulfuric acid; hydrogen bromide; at 80 ℃; Rate constant; effect of reagent concentrations; influence of acidity of medium; concentration equilibrium constant; densities at 25 deg C of the initial reaction mixture and the reaction mixture obtained at the end of the experiment;

DOI:10.1007/BF00954274

Reference yield:

sulfuric acid monopropyl ester (13425-84-8) → propan-1-ol (71-23-8)

Guidance literature:

With sulfuric acid; at 32.5 ℃; Equilibrium constant;

upstream raw materials:

propan-1-ol

diammonium salt of phenyl phosphatosulfate

Downstream raw materials:

1-propyl-2-(2-hydroxyethyl)piperidine

propyl 2-phenylquinoline-4-carboxylate

6-methyl-2-phenyl-quinoline-4-carboxylic acid propyl ester

propan-1-ol

Refernces

• 1、 Vinnik, M. I.,Skakun, S. A.,Shelud'ko, A. B.. "KINETICS OF THE HYDROBROMINATION OF n-PROPYL ALCOHOL BY HYDROGEN BROMIDE IN AQUEOUS SOLUTIONS OF HBr WITH H2SO4 CONTAINING HIGH CONCENTRATION OF ALCOHOL". . p. 1582 - 1588. Retrieved 2007/10/02.