Technology Process of 1-(Benzyloxy)-4-{(Z)-[4-(benzyloxy)phenyl]-NNO-azoxy}benzene
There total 5 articles about 1-(Benzyloxy)-4-{(Z)-[4-(benzyloxy)phenyl]-NNO-azoxy}benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,4,6-tri-tert-butylnitrobenzene radical anion * Li(1+);
In
dimethyl sulfoxide;
at 25 ℃;
for 864h;
DOI:10.1021/ja00270a021
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 82 percent / 25percent NaOH, Aliquat 360 / CH2Cl2; H2O / 5 h / 50 °C
2: 15 percent / 2,4,6-tri-tert-butylnitrobenzene radical anion * Li(1+) / dimethylsulfoxide / 864 h / 25 °C
With
sodium hydroxide; 2,4,6-tri-tert-butylnitrobenzene radical anion * Li(1+); Aliquat 360;
In
dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja00270a021
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 82 percent / 25percent NaOH, Aliquat 360 / CH2Cl2; H2O / 5 h / 50 °C
2: 15 percent / 2,4,6-tri-tert-butylnitrobenzene radical anion * Li(1+) / dimethylsulfoxide / 864 h / 25 °C
With
sodium hydroxide; 2,4,6-tri-tert-butylnitrobenzene radical anion * Li(1+); Aliquat 360;
In
dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja00270a021