Acetic acid, praseodymium(3+) salt, trihydrate

Base Information

• Chemical Name: Acetic acid, praseodymium(3+) salt, trihydrate
• CAS No.: 14431-99-3
• Molecular Formula: C2H4O2.H2O.1/3Pr
• Mol file: 14431-99-3.mol

Synonyms:

Chemical Property of Acetic acid, praseodymium(3+) salt, trihydrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid, praseodymium(3+) salt, trihydrate

There total 4 articles about Acetic acid, praseodymium(3+) salt, trihydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

praseodymium(III) oxide → Pr(OAc)3(H2O) (14431-99-3,17829-83-3,25721-94-2,28016-26-4,71546-14-0)

Guidance literature:

With water; acetic acid; slight excess of the oxide boiled with a mixture of water and EtOH (1/1); excess oxide removed by filtration, soln. left to crystallize, recrystd. from 2% CH3COOH;

DOI:10.1021/ja00069a034

Reference yield:

praseodymium(III) chloride heptahydrate (10025-90-8,17272-46-7,19423-77-9) → Pr(OAc)3(H2O) (14431-99-3,17829-83-3,25721-94-2,28016-26-4,71546-14-0)

Guidance literature:

With ammonia; acetic acid; In water; PrCl3*7H2O dissolved in water, NH3 added dropwise; filtered, redissolved by glacial acetic acid, repeated three times, X-ray powder diffraction;

Reference yield:

praseodymium(III) nitrate → Pr(OAc)3(H2O) (14431-99-3,17829-83-3,25721-94-2,28016-26-4,71546-14-0)

Guidance literature:

With sodium acetate; In water; addn. of stoich. amount of sodium acetate to aq. soln. of rare earth nitrate; ppt. filtration off, washing (water), drying (air, 50°C, 4 h); chem. anal.;

DOI:10.1016/S0020-1693(00)85449-3

upstream raw materials:

praseodymium(III) chloride heptahydrate

1-ethyl-3-methylimidazolium acetate

Refernces

• 1、 Bousrez, Guillaume,Renier, Olivier,Kelley, Steven P.,Adranno, Brando,Tahavori, Elnaz,Titi, Hatem M.,Smetana, Volodymyr,Tang, Si-Fu,Mudring, Anja-Verena,Rogers, Robin D.. "Ready Access to Anhydrous Anionic Lanthanide Acetates by Using Imidazolium Acetate Ionic Liquids as the Reaction Medium". . p. 13181 - 13189. Retrieved 2021/08/16.
• 2、 Hehlen, Markus P.,Riesen, Hans,Güdel, Hans U.. "Synthesis and spectroscopic properties of praseodymium(III) acetate hydrate". . p. 2273 - 2277. Retrieved 2008/10/08.