Technology Process of Sodium disulfide
There total 44 articles about Sodium disulfide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzyl chloride;
In
1,2-dimethoxyethane;
S8 was reacted with 2.2 at. equiv. of sodium dispersion in 1,2-dimethoxyethane under reflux for 5 h before treatment with 1.5 equiv. of benzyl chloride at room temp. for 1 h; selectivity of monosulfide >99%; catalystphenanthrene-0.18 equiv. toward Na; dibenzyl oligosulfane was studied by GC-MS and (1)H NMR spectra;
DOI:10.1021/ic034084z
- Guidance literature:
-
In
water;
Irradiation (UV/VIS); Hg-arc;
DOI:10.1038/137071a0
- Guidance literature:
-
With
pyrographite;
In
neat (no solvent);
byproducts: Co, CO2; reduction of Na2SO4 by C at deep red heat; product mixture is obtained;;
