Technology Process of (NZ)-N-[(4-phenylphenyl)methylidene]hydroxylamine
There total 4 articles about (NZ)-N-[(4-phenylphenyl)methylidene]hydroxylamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium carbonate;
In
methanol; water;
at 20 ℃;
for 3h;
DOI:10.1039/c6ra02222g
- Guidance literature:
-
4-bromo-1,1'-biphenyl;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -50 ℃;
for 0.5h;
Inert atmosphere;
N,N-dimethyl-formamide;
In
tetrahydrofuran; hexane;
at -50 - 20 ℃;
for 1h;
Inert atmosphere;
With
hydroxylamine hydrochloride; potassium carbonate;
In
tetrahydrofuran; hexane;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1016/j.tet.2018.06.044
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium chlorochromate; magnesium sulfate / chloroform / 3 h / Sealed tube
2: hydroxylamine hydrochloride; sodium acetate / water; ethanol; tetrahydrofuran / 72 h / 20 °C
With
hydroxylamine hydrochloride; sodium acetate; magnesium sulfate; pyridinium chlorochromate;
In
tetrahydrofuran; ethanol; chloroform; water;
DOI:10.1016/j.tetlet.2015.12.038