3,9-Diphenyl-2,4,8,10-tetraoxaspiro[5.5]undecane

Base Information

• Chemical Name: 3,9-Diphenyl-2,4,8,10-tetraoxaspiro[5.5]undecane
• CAS No.: 2064-95-1
• Molecular Formula: C19H20O4
• Molecular Weight: 312.365
• Hs Code.: 2932999099
• NSC Number: 48282
• DSSTox Substance ID: DTXSID40286927
• Nikkaji Number: J1.094.719G
• Wikidata: Q82022784
• ChEMBL ID: CHEMBL1332781
• Mol file: 2064-95-1.mol

Synonyms:3,9-diphenyl-2,4,8,10-tetraoxaspiro[5.5]undecane;2064-95-1;2,4,8,10-Tetraoxaspiro[5.5]undecane, 3,9-diphenyl-;NSC48282;Dibenzylidenpentaerythrit;Maybridge3_004529;MLS000573809;SCHEMBL764123;CHEMBL1332781;DTXSID40286927;DZQLZCHEALBORZ-UHFFFAOYSA-N;HMS1443N19;HMS2388O18;CAA06495;(1-pyridinylpiperidin-4-yl)methanol;CCG-17798;NSC-48282;AKOS001629107;IDI1_015916;SMR000184661;CS-0333662;FT-0741859;SR-01000453409;3,9-Diphenyl-2,4,8,10-tetraoxaspiro[5,5]undecan;SR-01000453409-1;SR-01000453409-2;2,8,10-Tetraoxaspiro[5.5]undecane, 3,9-diphenyl-

Chemical Property of 3,9-Diphenyl-2,4,8,10-tetraoxaspiro[5.5]undecane

Chemical Property:

• Vapor Pressure: 1.29E-08mmHg at 25°C
• Refractive Index: 1.6
• Boiling Point: 471.7 °C at 760 mmHg
• Flash Point: 160.6 °C
• PSA: 36.92000
• Density: 1.23 g/cm³
• LogP: 3.46400
• Storage Temp.: 2-8°C
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 312.13615911
• Heavy Atom Count: 23
• Complexity: 318

Purity/Quality:

98%,99%, ^*data from raw suppliers

3,9-diphenyl-2,4,8,10-tetraoxaspiro[5.5]undecane 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C2(COC(O1)C3=CC=CC=C3)COC(OC2)C4=CC=CC=C4
• Use Description: 3,9-diphenyl-2,4,8,10-tetraoxaspiro[5.5]undecane, a chemical compound with a unique and complex structure, has several applications across different fields. In the field of organic chemistry, it serves as a valuable building block for the synthesis of various organic compounds, including pharmaceuticals, agrochemicals, and specialty chemicals. Its versatile reactivity enables chemists to create intricate molecular structures, making it a crucial component of drug development and chemical research. Additionally, in materials science, this compound can be used in the formulation of polymers, resins, and adhesives, enhancing their properties and performance. Moreover, its potential role in the development of novel materials for electronic and optical applications is an area of ongoing research. Overall, 3,9-diphenyl-2,4,8,10-tetraoxaspiro[5.5]undecane plays a pivotal role in advancing chemistry, materials science, and various industries through its diverse applications.

Technology Process of 3,9-Diphenyl-2,4,8,10-tetraoxaspiro[5.5]undecane

There total 10 articles about 3,9-Diphenyl-2,4,8,10-tetraoxaspiro[5.5]undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Pentaerythritol (115-77-5) + benzaldehyde (100-52-7) → 3,9-diphenyl-2,4,8,10-tetraoxa-spiro[5,5]undecane (2064-95-1)

Guidance literature:

With pyrographite; In benzene; for 1.5h; Heating;

DOI:10.1080/00397919908086141

Reference yield: 98.0%

2,2-bis(hydroxymethyl)propane-1,3-diol (82515-50-2) + benzaldehyde (100-52-7) → 3,9-diphenyl-2,4,8,10-tetraoxa-spiro[5,5]undecane (2064-95-1)

Guidance literature:

With iron(II) sulfate; In toluene; for 0.8h; Heating;

DOI:10.1039/a900025i

Reference yield: 96.0%

Pentaerythritol (115-77-5) + benzaldehyde dimethyl acetal (1125-88-8) → 3,9-diphenyl-2,4,8,10-tetraoxa-spiro[5,5]undecane (2064-95-1)

Guidance literature:

With tetrachlorosilane; In acetonitrile; at 20 ℃;

DOI:10.1080/10426500214879

upstream raw materials:

Pentaerythritol

(diethoxymethyl)benzene

benzaldehyde

2,2-bis(hydroxymethyl)propane-1,3-diol

Downstream raw materials:

pyrographite

2,2-Di(benzyloxymethyl)-1,3-propandiyl tetradecanoate

2,2-Di(hydroxymethyl)-1,3-propandiyl tetradecanoate

2-phenyl-1,3-dithiane

Refernces

• 1、 Lizarzaburu, Mike E.,Jones, Ryan M.,Nantz, Michael H.,Kurth, Mark J.. "Multi-gram synthesis of dimyristoyl pentaerythritol". . p. 440 - 442. Retrieved 1999.
• 2、 Zhang, Yunjuan,Luo, Peng,Xu, Hao,Han, Lu,Wu, Peng,Sun, Huai,Che, Shunai. "Hierarchical MFI Zeolites with a Single-Crystalline Sponge-Like Mesostructure". supporting information. p. 19300 - 19308. Retrieved 2018/11/27.