Technology Process of Ethanone, 1-[3,4-dimethoxy-6-(phenylmethoxy)-2-(1-propenyl)phenyl]-
There total 1 articles about Ethanone, 1-[3,4-dimethoxy-6-(phenylmethoxy)-2-(1-propenyl)phenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
/BRN= 3312879/;
- Guidance literature:
-
With
magnesium; magnesium bromide; lithium diisopropyl amide;
In
tetrahydrofuran;
-78 degC, 1 h then -78 degC, 3 h;
DOI:10.1039/P19870000389
- Guidance literature:
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Multi-step reaction with 12 steps
2: 1.) N-chlorosuccinimide, dimethyl sulphide, 2.) Zn / 2.) acetic acid
3: 87 percent / dioxane
4: sodium metaperiodate
5: 5percent H2SO4-AcOH / tetrahydrofuran / 3 h / Heating
7: 1.) H2, 5percent HCl, 2.) O3 / 1.) r.t., 4 d
8: 1.) O3, 2.) Me2S
9: sulphamic acid, sodium chlorite
10: H2SO4 / acetone
11: 52 percent / AlCl3, Me2S / CH2Cl2 / -10 °C
12: 68 percent / 5percent HCl / acetone / 24 h / 55 °C
With
hydrogenchloride; sodium chlorite; sodium periodate; N-chloro-succinimide; aluminium trichloride; dimethylsulfide; sulfuric acid; aminosulfonic acid; hydrogen; ozone; acetic acid; zinc;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; acetone;
DOI:10.1039/c39840001565
