TETRADECANOIC-13,13,14,14,14-D5 ACID

Base Information

• Chemical Name: TETRADECANOIC-13,13,14,14,14-D5 ACID
• CAS No.: 327077-03-2
• Molecular Formula: CD3(CH2)12COOH
• Molecular Weight: 231.39
• Mol file: 327077-03-2.mol

Synonyms:

Chemical Property of TETRADECANOIC-13,13,14,14,14-D5 ACID

Chemical Property:

• Melting Point: 52-54oC(lit.)
• Boiling Point: 250oC/100 mmHg(lit.)
• PSA: 37.30000
• LogP: 4.77210

Purity/Quality:

TetradecanoicAcid-13,13,14,14,14-d5 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Tetradecanoic-13,13,14,14,14-d5 Acid (CAS# 327077-03-2) is a useful isotopically labeled research compound.

Technology Process of TETRADECANOIC-13,13,14,14,14-D5 ACID

There total 24 articles about TETRADECANOIC-13,13,14,14,14-D5 ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C14H23(2)H7O → erythro-(11,12,13,13,14,14,14-2H7)myristic acid (327077-03-2,358730-97-9)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In water;

DOI:10.1021/ja972577v

Reference yield: 96.0%

C14H23(2)H7O → threo-(11,12,13,13,14,14,14-2H7)myristic acid (327077-03-2,358730-97-9)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In water;

DOI:10.1021/ja972577v

Reference yield: 85.0%

[13,13,14,14,14-(2)H5]-tetradecan-1-ol (948862-51-9) → [13,13,14,14,14-d5]-tetradecanoic acid (327077-03-2)

Guidance literature:

With Jones reagent; In acetone; at 0 ℃; for 4h;

DOI:10.1002/jlcr.1666

upstream raw materials:

n-tetradecanoic acid

1-methoxymethyloxy-11-dodecyne

[13,13,14,14,14-⁽²⁾H₅]-(Z)-11-tetradecen-1-ol

(1,1,2,2,2-⁽²⁾H₅) (Z)-15,17-dioxa-3-octadecene

Refernces

• 1、 Navarro, Isabel,Fabrias, Gemma,Camps, Francisco. "Insect desaturases as unique analytical tools to unravel the stereochemical course of the reduction of vicinal ditosylates with lithium aluminum deuteride". . p. 164 - 166. Retrieved 2007/10/03.
• 2、 Bersch, B.,Starck, J. P.,Milon, A.,Nakatani, Y.,Ourisson, G.. "Total synthesis of perdeuterated phospholipids". . p. 575 - 583. Retrieved 2007/10/02.