ethyl bis-(4-nitrophenyl)acetate

Base Information

• Chemical Name: ethyl bis-(4-nitrophenyl)acetate
• CAS No.: 40748-64-9
• Molecular Formula: C₁₆H₁₄N₂O₆
• Molecular Weight: 330.297
• Mol file: 40748-64-9.mol

Synonyms:ethyl bis-(4-nitrophenyl)acetate

Chemical Property of ethyl bis-(4-nitrophenyl)acetate

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl bis-(4-nitrophenyl)acetate

There total 6 articles about ethyl bis-(4-nitrophenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Ethoxy-2,2-bis-(4-nitro-phenyl)-ethenol; compound with N,N,N',N'-tetramethyl-guanidine → ethyl bis-(4-nitrophenyl)acetate (40748-64-9) + N,N,N',N'-tetramethylguanidine (80-70-6)

Guidance literature:

In tetrahydrofuran; at 10.3 - 34.8 ℃; Kinetics; Equilibrium constant;

DOI:10.1039/P29790001099

Reference yield:

ethyl acetoacetate (141-97-9) + 4-chlorobenzonitrile (100-00-5) → ethyl bis-(4-nitrophenyl)acetate (40748-64-9)

Guidance literature:

With sodium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide;

DOI:10.1021/jo00957a018

Reference yield:

ethyl diphenylacetate (3468-99-3) → ethyl bis-(4-nitrophenyl)acetate (40748-64-9)

Guidance literature:

With nitric acid; at -30 ℃;

DOI:10.1039/jr9520002806

upstream raw materials:

ethyl diphenylacetate

ethyl acetoacetate

4-chlorobenzonitrile

1,1,1-trifluoro-2,2-bis-(4-nitrophenyl) ethane

Downstream raw materials:

N₁,N₁,N₃,N₃-tetramethylguanidinium

Refernces