N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine

Base Information

• Chemical Name: N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine
• CAS No.: 74114-75-3
• Molecular Formula: C₁₁H₁₆N₂O₄S
• Molecular Weight: 272.325
• Mol file: 74114-75-3.mol

Synonyms:N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine

Chemical Property of N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine

There total 2 articles about N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butoxycarbonylhydrazine (870-46-2) + benzenesulfonyl chloride (98-09-9) → N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine (74114-75-3)

Guidance literature:

With pyridine; In diethyl ether; 1.) 1 h, ice cooled, 2.) 1 h, room temp.;

DOI:10.1055/s-1980-28986

Reference yield:

→ N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine (74114-75-3)

Guidance literature:

Reference yield: 84.0%

N-benzene sulfonyl-N'-carbo-tert-butoxy hydrazine (74114-75-3) → benzenesufonyl hydrazide (80-17-1)

Guidance literature:

With trifluoroacetic acid; for 0.5h;

DOI:10.1002/jccs.200700220

upstream raw materials:

t-butoxycarbonylhydrazine

benzenesulfonyl chloride

Downstream raw materials:

benzenesufonyl hydrazide

Refernces

• 1、 Gordon, Michael S.,Krause, Josef G.,Linneman-Mohr, Michelle A.,Parchue, Regis R.. "Hydrazides and Hydrazones from Carbazates". . p. 244 - 245. Retrieved 2007/10/02.