4-bromo-2,3-dimethylaniline hydrobromide

Base Information

• Chemical Name: 4-bromo-2,3-dimethylaniline hydrobromide
• CAS No.: 1338796-79-4
• Molecular Formula: BrH*C₈H₁₀BrN
• Molecular Weight: 280.99
• Mol file: 1338796-79-4.mol

Synonyms:4-bromo-2,3-dimethylaniline hydrobromide

Chemical Property of 4-bromo-2,3-dimethylaniline hydrobromide

Chemical Property:

Purity/Quality:

97% or 98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-bromo-2,3-dimethylaniline hydrobromide

There total 1 articles about 4-bromo-2,3-dimethylaniline hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,3-Dimethylaniline (87-59-2) → 4-bromo-2,3-dimethylaniline hydrobromide (1338796-79-4)

Guidance literature:

With tetra-N-butylammonium tribromide; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.06.089

Reference yield: 78.0%

4-bromo-2,3-dimethylaniline hydrobromide (1338796-79-4) → 4-bromo-2,3-dimethylbenzenediazonium tetrafluoroborate

Guidance literature:

With tetrafluoroboric acid; tert.-butylnitrite; In water; acetonitrile; at -20 ℃; for 0.75h;

DOI:10.1016/j.bmc.2011.06.089

Reference yield:

4-bromo-2,3-dimethylaniline hydrobromide (1338796-79-4) → 1,4-dibromo-2,3-dimethylbenzene (75024-22-5)

Guidance literature:

4-bromo-2,3-dimethylaniline hydrobromide; With sodium carbonate; In diethyl ether; water;

With tert.-butylnitrite; copper(ll) bromide; In acetonitrile; at 20 - 82 ℃; for 20h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.06.089

upstream raw materials:

2,3-Dimethylaniline

Downstream raw materials:

4-bromo-7-(tert-butoxycarbonylamino)-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one

1-bromo-4-phenyl-7-tert-butyloxycarbonylamino-5,7,8,9-tetrahydro-benzocyclohepten-6-one

7-amino-4-bromo-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one hydrochloride

1-bromo-4-phenyl-7-amino-5,7,8,9-tetrahydro-6H-benzocyclohepten-6-one hydrochloride

Refernces