N²-benzyloxycarbonyl-N⁶-[5-((3aS)-2-oxo-(3ar,6ac)-hexahydro-thieno[3,4-d]imidazol-4t-yl)-pentanoyl]-L-lysine amide

Base Information

• Chemical Name: N²-benzyloxycarbonyl-N⁶-[5-((3aS)-2-oxo-(3ar,6ac)-hexahydro-thieno[3,4-d]imidazol-4t-yl)-pentanoyl]-L-lysine amide
• CAS No.: 67917-55-9
• Molecular Formula: C₂₄H₃₅N₅O₅S
• Molecular Weight: 505.638
• Mol file: 67917-55-9.mol

Synonyms:N²-benzyloxycarbonyl-N⁶-[5-((3aS)-2-oxo-(3ar,6ac)-hexahydro-thieno[3,4-d]imidazol-4t-yl)-pentanoyl]-L-lysine amide

Chemical Property of N²-benzyloxycarbonyl-N⁶-[5-((3aS)-2-oxo-(3ar,6ac)-hexahydro-thieno[3,4-d]imidazol-4t-yl)-pentanoyl]-L-lysine amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N²-benzyloxycarbonyl-N⁶-[5-((3aS)-2-oxo-(3ar,6ac)-hexahydro-thieno[3,4-d]imidazol-4t-yl)-pentanoyl]-L-lysine amide

There total 1 articles about N²-benzyloxycarbonyl-N⁶-[5-((3aS)-2-oxo-(3ar,6ac)-hexahydro-thieno[3,4-d]imidazol-4t-yl)-pentanoyl]-L-lysine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N2-benzyloxycarbonyl-L-lysine amide; trifluoroacetate (67917-54-8) + biotin (58-85-5,22879-79-4) → N2-benzyloxycarbonyl-N6-[5-((3aS)-2-oxo-(3ar,6ac)-hexahydro-thieno[3,4-d]imidazol-4t-yl)-pentanoyl]-L-lysine amide (67917-55-9)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1021/ja00479a048

Reference yield:

N2-benzyloxycarbonyl-N6-[5-((3aS)-2-oxo-(3ar,6ac)-hexahydro-thieno[3,4-d]imidazol-4t-yl)-pentanoyl]-L-lysine amide (67917-55-9) → Biocytinamid (61125-53-9)

Guidance literature:

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium; In water; N,N-dimethyl-formamide;

DOI:10.1021/ja00479a048

upstream raw materials:

N²-benzyloxycarbonyl-L-lysine amide; trifluoroacetate

biotin

Downstream raw materials:

Biocytinamid