Anthra[2,1,9-mna]naphth[2,3-h]acridine-5,10,15(16H)-trione

Base Information

• Chemical Name: Anthra[2,1,9-mna]naphth[2,3-h]acridine-5,10,15(16H)-trione
• CAS No.: 3271-76-9
• Deprecated CAS: 1328-45-6
• Molecular Formula: C31H15NO3
• Molecular Weight: 449.465
• Hs Code.: 2933990090
• European Community (EC) Number: 221-897-7,603-679-7
• DSSTox Substance ID: DTXSID3062944
• Nikkaji Number: J34.099E
• Wikidata: Q72516166
• Mol file: 3271-76-9.mol

Synonyms:Vat Green 3;3271-76-9;Vat Olive Green B;Cibanone Olive B;Tinon Olive B;Cibanone Olive FB;Ponsol Green 2BL;Cibanone Olive 2B;Anthra[2,1,9-mna]naphth[2,3-h]acridine-5,10,15(16H)-trione;Ponsol Green 2BLD;Cibanone Olive 2BD;Mayvat Olive Green B;Caledon Olive Green B;C.I. Vat Green 3;Ahcoval Olive Green BL;Benzadone Olive Green B;Sandothrene Olive N 2B;Atic Vat Olive Green B;Tyrian Olive Green I-B;Ahcoval Olive Green BLD;Amanthrene Olive Green B;Fenanthren Olive Green B;Indanthren Olive Green B;Mikethrene Olive Green B;Nyanthrene Olive Green B;Ostanthren Olive Green B;Solanthrene Dark Green J;Calcoloid Olive Green BD;Calcoloid Olive Green BN;Zelen kypova 3 [Czech];Arlanthrene Olive Green B;Belanthrene Olive Green B;Helanthrene Olive Green B;Indanthrene Olive Green B;Nihonthrene Olive Green B;Palanthrene Olive Green B;Pernithrene Olive Green B;Ahcoval Olive Green BL-F;Calcoloid Olive Green BDC;Calcoloid Olive Green BDL;Calcoloid Olive Green BNC;Carbanthrene Olive Green B;Zelen kypova 3;Indanthrene Olive Green BA;Romanthrene Olive Green FB;Solanthrene Dark Green F-J;Amanthrene Supra Olive Green B;Caledon Printing Olive Green B;Ahcoval Printing Olive Green BL;EINECS 221-897-7;Zelen olivova ostanthrenova B [Czech];BRN 0060973;Zelen olivova ostanthrenova B;C.I. 69500;C.I. 70311;Anthra(2,1,9-mna)naphth(2,3-h)acridine-5,10,15(16H)-trione;0-21-00-00571 (Beilstein Handbook Reference);27-hydroxy-16-azaoctacyclo[18.10.2.02,15.05,14.07,12.017,31.021,26.028,32]dotriaconta-1,3,5(14),7,9,11,15,17(31),18,20(32),21,23,25,27,29-pentadecaene-6,13-dione;SCHEMBL458628;DTXSID3062944;C31H15NO3;Anthra[2,1,9-mna]naphth[2, 3-h]acridine-5,10,15(16H)-trione;C31-H15-N-O3;LS-20416

Chemical Property of Anthra[2,1,9-mna]naphth[2,3-h]acridine-5,10,15(16H)-trione

Chemical Property:

• Vapor Pressure: 9.27E-24mmHg at 25°C
• Refractive Index: 1.806
• Boiling Point: 772 °C at 760 mmHg
• PKA: -2.68±0.20(Predicted)
• Flash Point: 261.3 °C
• PSA: 64.10000
• Density: 1.48 g/cm³
• LogP: 1.85540
• Water Solubility.: 0.03ng/L at 20℃
• XLogP3: 7.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 449.10519334
• Heavy Atom Count: 35
• Complexity: 902

Purity/Quality:

99.9% ^*data from raw suppliers

VAT GREEN 3 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=C4C(=C2O)C=CC5=C6C=CC7=C(C6=NC(=C54)C=C3)C(=O)C8=CC=CC=C8C7=O

Technology Process of Anthra[2,1,9-mna]naphth[2,3-h]acridine-5,10,15(16H)-trione

There total 3 articles about Anthra[2,1,9-mna]naphth[2,3-h]acridine-5,10,15(16H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromobenzanthrone (81-96-9) + 1-amino-9,10-anthracenedione (82-45-1) → Vat Dark Green Zh (3271-76-9)

Guidance literature:

3-bromobenzanthrone; 1-amino-9,10-anthracenedione; With sodium carbonate; copper(II) oxide; In nitrobenzene; at 210 ℃; for 2h; Industrial scale;

With potassium hydroxide; sodium hydroxide; In water; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; at 150 ℃; for 4h; Reagent/catalyst; Temperature; Catalytic behavior; Industrial scale;

Reference yield:

1-[(7-oxo-7H-benz[de]anthracene-3-yl)amino]anthraquinone (81-94-7) → Vat Dark Green Zh (3271-76-9)

Guidance literature:

With potassium hydroxide; at 240 - 245 ℃; durch Schmelzen und Kochen des Reaktionsprodukts mit Wasser und Behandeln der Loesung mit Luft;

Reference yield:

→ Vat Dark Green Zh (3271-76-9)

Guidance literature:

kommerzielles Romantrene Olive Green B;

upstream raw materials:

1-[(7-oxo-7H-benz[de]anthracene-3-yl)amino]anthraquinone

3-bromobenzanthrone

1-amino-9,10-anthracenedione

Refernces