Technology Process of C23H20N3O3P
There total 1 articles about C23H20N3O3P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: caesium carbonate / tetrahydrofuran; isopropyl alcohol
2: hydrogenchloride / water
3: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 75 °C
4: ammonium acetate; ammonium hydroxide; zinc / ethanol; water / 80 °C
5: N-ethyl-N,N-diisopropylamine / dichloromethane
6: trichlorophosphate / 100 °C
7: ammonia / methanol
8: trifluoroacetic anhydride / tetrahydrofuran; pyridine
9: hydrazine hydrate / methanol
10: 120 °C
With
hydrogenchloride; hydroxylamine hydrochloride; ammonium acetate; ammonia; caesium carbonate; ammonium hydroxide; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; sodium hydroxide; zinc; trichlorophosphate;
In
tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; water; isopropyl alcohol;
1: Horner-Emmons condensation;
DOI:10.1016/j.bmcl.2011.08.071
- Guidance literature:
-
Multi-step reaction with 2 steps
1: caesium carbonate / tetrahydrofuran; isopropyl alcohol
2: hydrogenchloride / water
With
hydrogenchloride; caesium carbonate;
In
tetrahydrofuran; water; isopropyl alcohol;
1: Horner-Emmons condensation;
DOI:10.1016/j.bmcl.2011.08.071