bis(2-methylphenyl)borinic acid

Base Information Edit

Chemical Name:bis(2-methylphenyl)borinic acid
CAS No.:73774-44-4
Molecular Formula:C₁₄H₁₅BO
Molecular Weight:210.084
Hs Code.:
Mol file:73774-44-4.mol

Synonyms:bis(2-methylphenyl)borinic acid

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Chemical Property of bis(2-methylphenyl)borinic acid Edit

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Technology Process of bis(2-methylphenyl)borinic acid

There total 6 articles about bis(2-methylphenyl)borinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 97881-32-8
2-(di-o-tolyl-boranyloxy)-ethylamine

: 73774-44-4
bis(2-methylphenyl)borinic acid

Guidance literature:: With hydrogenchloride; In methanol; acetone; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c5cc06177f

Reference yield:

: 95-46-5
2-methylphenyl bromide

: 73774-44-4
bis(2-methylphenyl)borinic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: boric acid tributyl ester; magnesium; iodine / tetrahydrofuran / 40 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride / water

With hydrogenchloride; boric acid tributyl ester; iodine; magnesium; In tetrahydrofuran; water;
DOI:10.1021/jo301335x