1-methyl-1-(3-methylamino-2-nitroacryloyl)-3-(p-nitro-phenyl)urea methylammonium salt

Base Information

• Chemical Name: 1-methyl-1-(3-methylamino-2-nitroacryloyl)-3-(p-nitro-phenyl)urea methylammonium salt
• CAS No.: 128039-12-3
• Molecular Formula: CH₅N*C₁₂H₁₃N₅O₆
• Molecular Weight: 354.323
• Mol file: 128039-12-3.mol

Synonyms:1-methyl-1-(3-methylamino-2-nitroacryloyl)-3-(p-nitro-phenyl)urea methylammonium salt

Chemical Property of 1-methyl-1-(3-methylamino-2-nitroacryloyl)-3-(p-nitro-phenyl)urea methylammonium salt

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-methyl-1-(3-methylamino-2-nitroacryloyl)-3-(p-nitro-phenyl)urea methylammonium salt

There total 1 articles about 1-methyl-1-(3-methylamino-2-nitroacryloyl)-3-(p-nitro-phenyl)urea methylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

3-methyl-5-nitro-1-(p-nitrophenyl)uracil (108047-30-9) + methylamine (74-89-5) → 1-methyl-1-(3-methylamino-2-nitroacryloyl)-3-(p-nitro-phenyl)urea methylammonium salt (128039-12-3)

Guidance literature:

In methanol; ethanol; for 0.0166667h; Product distribution; Ambient temperature; other object, other cond.: dimethylamine, water, ethanol, 4h, roomtemp.;

DOI:10.1039/P19900000367

Reference yield: 99.0%

1-methyl-1-(3-methylamino-2-nitroacryloyl)-3-(p-nitro-phenyl)urea methylammonium salt (128039-12-3) → 3-methyl-5-nitro-1-(p-nitrophenyl)uracil (108047-30-9)

Guidance literature:

With hydrogenchloride; In ethanol; water; for 0.0166667h; Ambient temperature;

DOI:10.1039/P19900000367

Reference yield: 92.0%

1-methyl-1-(3-methylamino-2-nitroacryloyl)-3-(p-nitro-phenyl)urea methylammonium salt (128039-12-3) → 1,3-dimethyl-5-nitrouracil (41613-26-7)

Guidance literature:

With triethylamine; In ethanol; for 6h; Ambient temperature; ethanol, 5 min, reflux;

DOI:10.1039/P19900000367

upstream raw materials:

3-methyl-5-nitro-1-(p-nitrophenyl)uracil

methylamine

Downstream raw materials:

1,3-dimethyl-5-nitrouracil

3-methyl-5-nitro-1-(p-nitrophenyl)uracil

1-ethyl-3-methyl-5-nitrouracil

3-methyl-5-nitro-2,4(1H,3H)pyrimidinedione

Refernces