Technology Process of C36H24
There total 3 articles about C36H24 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate;
In
tetrahydrofuran; ethanol; water;
at 75 ℃;
for 5h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide / chlorobenzene; N,N-dimethyl-formamide / 3 h / 85 °C
2: tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate / ethanol; water; tetrahydrofuran / 5 h / 75 °C / Inert atmosphere
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; chlorobenzene;
2: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate / ethanol; water; tetrahydrofuran / 14 h / 75 °C / Inert atmosphere
2: N-Bromosuccinimide / chlorobenzene; N,N-dimethyl-formamide / 3 h / 85 °C
3: tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate / ethanol; water; tetrahydrofuran / 5 h / 75 °C / Inert atmosphere
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; chlorobenzene;
1: |Suzuki Coupling / 3: |Suzuki Coupling;