Technology Process of C62H72N2
There total 5 articles about C62H72N2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine;
In
toluene;
at 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene / 40 h / 100 °C / Inert atmosphere
2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 16 h / 80 °C
3: sodium carbonate; Aliquat 336 / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 42 h / 90 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane / 20 °C
5: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 20 °C / Inert atmosphere
With
potassium acetate; Aliquat 336; sodium carbonate; trifluoroacetic acid; sodium t-butanolate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine;
In
dichloromethane; water; N,N-dimethyl-formamide; toluene;
3: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 16 h / 80 °C
2: sodium carbonate; Aliquat 336 / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 42 h / 90 °C / Inert atmosphere
3: trifluoroacetic acid / dichloromethane / 20 °C
4: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 20 °C / Inert atmosphere
With
potassium acetate; Aliquat 336; sodium carbonate; trifluoroacetic acid; sodium t-butanolate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine;
In
dichloromethane; water; N,N-dimethyl-formamide; toluene;
2: Suzuki Coupling;