Technology Process of C14H19NOSe
There total 4 articles about C14H19NOSe which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 93 percent / H2 / Pd/C / methanol / 6.5 h / 3102.9 Torr / Ambient temperature
2: 1.) (COCl)2, DMF, 2.) N-hydroxy-2-thiopyridone / 1.) CH2ClCH2Cl, room temperature, 12 h, 2.) CH2ClCH2Cl, room temperature, 1.5 h, 3.) CH2Cl2, irradiation, 0 deg C, 2 h
3: NaIO4 / H2O / 2 h / Ambient temperature
With
1-hydroxy-2(1H)-pyridinethione; sodium periodate; oxalyl dichloride; hydrogen; N,N-dimethyl-formamide;
palladium on activated charcoal;
In
methanol; water;
DOI:10.1021/jo980153t
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 86 percent / conc. HCl / 24 h / Heating
2: 93 percent / H2 / Pd/C / methanol / 6.5 h / 3102.9 Torr / Ambient temperature
3: 1.) (COCl)2, DMF, 2.) N-hydroxy-2-thiopyridone / 1.) CH2ClCH2Cl, room temperature, 12 h, 2.) CH2ClCH2Cl, room temperature, 1.5 h, 3.) CH2Cl2, irradiation, 0 deg C, 2 h
4: NaIO4 / H2O / 2 h / Ambient temperature
With
hydrogenchloride; 1-hydroxy-2(1H)-pyridinethione; sodium periodate; oxalyl dichloride; hydrogen; N,N-dimethyl-formamide;
palladium on activated charcoal;
In
methanol; water;
DOI:10.1021/jo980153t
- Guidance literature:
-
With
sodium periodate;
In
water;
for 2h;
Ambient temperature;
DOI:10.1021/jo980153t