3,5,5-trimethylhexanamide

Base Information

• Chemical Name: 3,5,5-trimethylhexanamide
• CAS No.: 90726-43-5
• Molecular Formula: C₉H₁₉NO
• Molecular Weight: 157.256
• Mol file: 90726-43-5.mol

Synonyms:3,5,5-trimethylhexanamide

Chemical Property of 3,5,5-trimethylhexanamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5,5-trimethylhexanamide

There total 2 articles about 3,5,5-trimethylhexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

3,5,5-trimethyl hexanal (5435-64-3) → 3,5,5-trimethylhexanamide (90726-43-5) + 3,5,5-trimethylhexanoic acid (3302-10-1)

Guidance literature:

With H₂SO₄*2NH₂OH; Rh(OH)x/Al₂O₃; In water; for 7h; Heating;

DOI:10.1002/anie.200701273

Reference yield: 60.0%

3,5,5-trimethylhexanoic acid (3302-10-1) → 3,5,5-trimethylhexylamine (3378-63-0) + 3,5,5-trimethylhexanamide (90726-43-5) + bis(3,5,5-trimethylhexyl)amine (926-75-0)

Guidance literature:

3,5,5-trimethylhexanoic acid; With cyclopentyl methyl ether; ammonia; at 200 ℃; under 4500.45 Torr; Sealed tube; Green chemistry;

With cyclopentyl methyl ether; ammonia; hydrogen; at 200 ℃; for 6.5h; under 42004.2 Torr; Cooling with ice; Green chemistry;

DOI:10.1039/d0gc01441a

upstream raw materials:

3,5,5-trimethyl hexanal

3,5,5-trimethylhexanoic acid

Refernces

• 1、 Fujiwara, Hiroshi,Ogasawara, Yoshiyuki,Yamaguchi, Kazuya,Mizuno, Noritaka. "A one-pot synthesis of primary amides from aldoximes or aldehydes in water in the presence of a supported rhodium catalyst". . p. 5202 - 5205. Retrieved 2008/03/13.