Technology Process of Niobium ethoxide
There total 13 articles about Niobium ethoxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
ethanol;
With
sodium;
In
hexane;
at -10 ℃;
for 4h;
Inert atmosphere;
Reflux;
niobium pentachloride tetrahydrofuran;
In
hexane;
at -10 ℃;
for 6h;
Reflux;
- Guidance literature:
-
With
LiCl;
In
water;
Electrochem. Process; anodic dissolution of Nb; 0.1 M LiCl-supporting electrolyte, at 35°C, Pt as cathode, anodic current density 0.03 A/cm**2; isolated by fractional distn.;
DOI:10.1134/S1070427206050090
- Guidance literature:
-
In
benzene;
introduction of dry NH3 into boiling soln. of NbCl5 in benzene containing CH3OH;; evaporization of soln.;;