C₂₂H₁₇NS

Base Information

• Chemical Name: C₂₂H₁₇NS
• CAS No.: 1085434-10-1
• Molecular Formula: C₂₂H₁₇NS
• Molecular Weight: 327.45
• Mol file: 1085434-10-1.mol

Synonyms:C₂₂H₁₇NS

Chemical Property of C₂₂H₁₇NS

Chemical Property:

• Boiling Point: 497.3±33.0 °C(Predicted)
• Density: 1.188±0.06 g/cm3(Predicted)

Purity/Quality:

≥99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₁₇NS

There total 1 articles about C₂₂H₁₇NS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

aniline (62-53-3) + 2-(4-bromophenyl)-5-phenylthiophene (118621-30-0) → C22H17NS (1085434-10-1)

Guidance literature:

aniline; 2-(4-bromophenyl)-5-phenylthiophene; With sodium t-butanolate; tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; for 2h; Heating / reflux;

With water; In toluene;

Reference yield: 65.0%

C22H17NS (1085434-10-1) + 1,5-dibromonaphthalene (7351-74-8) → C54H38N2S2 (1085434-34-9)

Guidance literature:

C₂₂H₁₇NS; 1,5-dibromonaphthalene; With sodium t-butanolate; tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; for 2h; Heating / reflux;

With water; In tetrahydrofuran; toluene; at 20 ℃;

Reference yield: 54.0%

C22H17NS (1085434-10-1) + 2-(3,5-dichlorophenyl)triphenylene → C68H46N2S2

Guidance literature:

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium t-butanolate; In 5,5-dimethyl-1,3-cyclohexadiene; for 7h; Inert atmosphere; Heating;

upstream raw materials:

aniline

2-(4-bromophenyl)-5-phenylthiophene

Downstream raw materials:

C₅₄H₃₈N₂S₂

Refernces

• 1、 -. "NEW DIAMINE DERIVATIVES AND ORGANIC ELECTRONIC DEVICE USING THE SAME". Page/Page column 52-53. . Retrieved 2008/12/08.