Technology Process of C18H19BrN2S
There total 3 articles about C18H19BrN2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(2-bromobenzyl)-1-butyl-1H-benzo[d]imidazol-3-ium bromide;
With
sodium disulfide;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
With
potassium tert-butylate;
In
tetrahydrofuran;
Inert atmosphere;
DOI:10.1016/j.jorganchem.2012.07.025
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1,4-dioxane / 16 h / Inert atmosphere; Reflux
2.1: sodium disulfide / tetrahydrofuran / 20 °C / Inert atmosphere
2.2: Inert atmosphere
With
sodium disulfide;
In
tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/j.jorganchem.2012.07.025
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydroxide; tetrabutylammomium bromide / water / 3 h / 55 °C / Inert atmosphere
2.1: 1,4-dioxane / 16 h / Inert atmosphere; Reflux
3.1: sodium disulfide / tetrahydrofuran / 20 °C / Inert atmosphere
3.2: Inert atmosphere
With
sodium disulfide; tetrabutylammomium bromide; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1016/j.jorganchem.2012.07.025