3-methoxy-3-phenypropenoate

Base Information

• Chemical Name: 3-methoxy-3-phenypropenoate
• CAS No.: 38750-49-1
• Molecular Formula: C₁₁H₁₂O₃
• Molecular Weight: 192.214
• Mol file: 38750-49-1.mol

Synonyms:3-methoxy-3-phenypropenoate

Chemical Property of 3-methoxy-3-phenypropenoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3-methoxy-3-phenypropenoate

There total 18 articles about 3-methoxy-3-phenypropenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.5%

methanol (67-56-1) + phenylpropynoic acid methyl ester (4891-38-7) → 3-methoxy-3-phenypropenoate (38750-49-1) + methyl 3-phenyl-3,3-dimethoxypropionate (116429-08-4)

Guidance literature:

With mercury(II) diacetate; toluene-4-sulfonic acid; at 53 ℃; for 72h; Title compound not separated from byproducts;

Reference yield: 21.0%

sodium methylate (124-41-4) + 3-((Z)-2-Methoxycarbonyl-1-phenyl-vinyl)-1-methyl-3H-imidazol-1-ium; iodide (91164-88-4) → 3-methoxy-3-phenypropenoate (38750-49-1)

Guidance literature:

In methanol; for 2h; Ambient temperature;

Reference yield: 21.0%

sodium methylate (124-41-4) + methyl 3-(2H-imidazol-1-yl)-3-phenylacrylate (85127-45-3) → 3-methoxy-3-phenypropenoate (38750-49-1)

Guidance literature:

In methanol; for 2h; Ambient temperature;

upstream raw materials:

methyl 3-phenyl-3,3-dimethoxypropionate

acetic anhydride

methanol

sodium methylate

Downstream raw materials:

methyl 3-oxo-3-phenylpropionate

acetophenone

3-methoxy-3-phenylpropenic acid

Refernces

• 1、 Kashima, Choji,Tajima, Tadakuni,Omote, Yoshimori. "The Compounds Related to 3-(1-Imidazolyl)-2-alken-1-ones. Preparation and Reactions". . p. 171 - 176. Retrieved 2007/10/02.