2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-YL)ethyl acetate

Base Information

• Chemical Name: 2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-YL)ethyl acetate
• CAS No.: 177950-06-0
• Molecular Formula: C₁₀H₁₉BO₄
• Molecular Weight: 214.069
• DSSTox Substance ID: DTXSID50700043
• Wikidata: Q82631214
• Mol file: 177950-06-0.mol

Synonyms:177950-06-0;2-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)ETHYL ACETATE;starbld0017033;DTXSID50700043;SLSUWTOYGHJHCJ-UHFFFAOYSA-N;EN300-4406842;2-(TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)ETHYL ACETATE;2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)ethyl acetate

Chemical Property of 2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-YL)ethyl acetate

Chemical Property:

• Boiling Point: 241.7±23.0 °C(Predicted)
• PSA: 44.76000
• Density: 1.00±0.1 g/cm3(Predicted)
• LogP: 1.64170
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 214.1376392
• Heavy Atom Count: 15
• Complexity: 234

Purity/Quality:

99% ^*data from raw suppliers

2-ACETOXYETHYLBORONIC ACID PINACOL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: B1(OC(C(O1)(C)C)(C)C)CCOC(=O)C

Technology Process of 2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-YL)ethyl acetate

There total 1 articles about 2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-YL)ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromoethyl acetate (927-68-4) + bis(pinacol)diborane (73183-34-3) → C10H19BO4 (177950-06-0)

Guidance literature:

With copper(l) iodide; lithium methanolate; In N,N-dimethyl-formamide; at 20 ℃; for 20h; Inert atmosphere;

DOI:10.1021/jo3021665

Reference yield: 40.0%

potassium hydrogen difluoride + C10H19BO4 (177950-06-0) → K(1+)*C4H7BF3O2(1-) (1408168-77-3)

Guidance literature:

In tetrahydrofuran; water; at 20 ℃; for 2h;

DOI:10.1021/jo3021665

upstream raw materials:

bromoethyl acetate

bis(pinacol)diborane

Downstream raw materials:

K⁽¹⁺⁾*C₄H₇BF₃O₂^(1-)

Refernces