Technology Process of C17H27NO3S
There total 5 articles about C17H27NO3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C10H18NO2S(1+)*ClO4(1-);
With
sodium hydroxide;
In
water; tert-butyl alcohol;
at 25 ℃;
for 1h;
Inert atmosphere;
1-cyclohexene-1-carboxaldehyde;
In
water; tert-butyl alcohol;
at 25 ℃;
Inert atmosphere;
DOI:10.1002/chem.201201332
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / dichloromethane / 0 °C / Inert atmosphere
2.1: sodium perchlorate / acetone / 40 °C / Inert atmosphere
3.1: sodium hydroxide / water; tert-butyl alcohol / 1 h / 25 °C / Inert atmosphere
3.2: 25 °C / Inert atmosphere
With
sodium perchlorate; triethylamine; sodium hydroxide;
In
dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1002/chem.201201332
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate; iodine / tetrahydrofuran / Reflux; Inert atmosphere
1.2: Reflux; Inert atmosphere
2.1: camphor-10-sulfonic acid / Molecular sieve; Reflux; Inert atmosphere
3.1: triethylamine / dichloromethane / 0 °C / Inert atmosphere
4.1: sodium perchlorate / acetone / 40 °C / Inert atmosphere
5.1: sodium hydroxide / water; tert-butyl alcohol / 1 h / 25 °C / Inert atmosphere
5.2: 25 °C / Inert atmosphere
With
sodium tetrahydroborate; camphor-10-sulfonic acid; sodium perchlorate; iodine; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1002/chem.201201332