4-(2-chloromercury-phenoxymethyl)-7,8-dimethyl-chromene-2-one

Base Information

• Chemical Name: 4-(2-chloromercury-phenoxymethyl)-7,8-dimethyl-chromene-2-one
• CAS No.: 1252026-25-7
• Molecular Formula: C₁₈H₁₅ClHgO₃
• Molecular Weight: 515.358
• Mol file: 1252026-25-7.mol

Synonyms:4-(2-chloromercury-phenoxymethyl)-7,8-dimethyl-chromene-2-one

Chemical Property of 4-(2-chloromercury-phenoxymethyl)-7,8-dimethyl-chromene-2-one

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-(2-chloromercury-phenoxymethyl)-7,8-dimethyl-chromene-2-one

There total 1 articles about 4-(2-chloromercury-phenoxymethyl)-7,8-dimethyl-chromene-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-(bromomethyl)-7,8-dimethyl-2H-chromen-2-one (1252026-46-2) + (2-hydroxyphenyl)mercury chloride (90-03-9) → 4-(2-chloromercury-phenoxymethyl)-7,8-dimethyl-chromene-2-one (1252026-25-7)

Guidance literature:

With potassium carbonate; In butanone; under N2; mixt. of 7,8-dimethyl-4-bromomethylcoumarin, o-chloromercury-phenol, anhyd. K2CO3 and dry butanone heated under reflux for 20-24 h; cooling to room temp., concn., soln. poured onto crushed ice, solid recrystd. from warm acetic acid; elem. anal.;

DOI:10.1016/j.poly.2010.07.010

upstream raw materials:

4-(bromomethyl)-7,8-dimethyl-2H-chromen-2-one

(2-hydroxyphenyl)mercury chloride

Refernces