N-Nitroso-N-benzylformamide

Base Information

• Chemical Name: N-Nitroso-N-benzylformamide
• CAS No.: 85995-49-9
• Molecular Formula: C₈H₈N₂O₂
• Molecular Weight: 164.164
• Mol file: 85995-49-9.mol

Synonyms:N-Nitroso-N-benzylformamide

Chemical Property of N-Nitroso-N-benzylformamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-Nitroso-N-benzylformamide

There total 1 articles about N-Nitroso-N-benzylformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzylformamide (6343-54-0) → N-Nitroso-N-benzylformamide (85995-49-9)

Guidance literature:

With nitrogen(II) oxide; acetic anhydride; acetic acid;

Reference yield: 62.0%

N-Nitroso-N-benzylformamide (85995-49-9) + diphenylmagnesium (555-54-4) → phenyl benzyl ketone (451-40-1) + benzophenone (119-61-9) + 1,1-Diphenylmethanol (91-01-0) + biphenyl (92-52-4,1594-86-1) + Benzyl acetate (140-11-4) + benzyl alcohol (100-51-6,185532-71-2)

Guidance literature:

With water; In diethyl ether; Product distribution; Ambient temperature;

DOI:10.1021/jo00163a012

Reference yield: 26.0%

N-Nitroso-N-benzylformamide (85995-49-9) + 4-methoxyphenyl magnesium bromide (13139-86-1) → benzyl bromide (100-39-0) + methoxybenzene (100-66-3)

Guidance literature:

In diethyl ether; at -3 - 0 ℃; for 1.5h; Product distribution; var. temp.;

DOI:10.1021/jo00163a012

upstream raw materials:

N-benzylformamide

Downstream raw materials:

phenyl benzyl ketone

benzophenone

1,1-Diphenylmethanol

biphenyl

Refernces