Technology Process of dibenzyl 2,2',3,3',4,4'-hexabenzyloxybiphenyl-6,6'-dicarboxylate
There total 6 articles about dibenzyl 2,2',3,3',4,4'-hexabenzyloxybiphenyl-6,6'-dicarboxylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium iodide; potassium hydroxide;
at 145 ℃;
for 4h;
Inert atmosphere;
DOI:10.1039/c0cc04007j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 32 percent / K2CO3, KI / various solvent(s) / 15 h / 140 °C
2: aq. KOH / ethanol / 2 h / Heating
3: K2CO3 / acetone / 4 h / Heating
With
potassium hydroxide; potassium carbonate; potassium iodide;
In
ethanol; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; sodium iodide / acetophenone / 18 h / 140 °C / Inert atmosphere
2: sodium iodide; potassium hydroxide / 4 h / 145 °C / Inert atmosphere
With
potassium carbonate; sodium iodide; potassium hydroxide;
In
acetophenone;
DOI:10.1039/c0cc04007j