o-Nitrobenzenesulfenylprolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

Base Information

• Chemical Name: o-Nitrobenzenesulfenylprolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester
• CAS No.: 88681-60-1
• Molecular Formula: C₃₁H₃₄N₄O₇S
• Molecular Weight: 606.7
• Mol file: 88681-60-1.mol

Synonyms:o-Nitrobenzenesulfenylprolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

Chemical Property of o-Nitrobenzenesulfenylprolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of o-Nitrobenzenesulfenylprolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

There total 1 articles about o-Nitrobenzenesulfenylprolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(S)-2-amino-5-benzyloxycarbonylamino-pentanoic acid benzyl ester hydrochloride (63594-37-6) + o-Nitrobenzenesulfenylproline 2,4,5-trichlorophenyl Ester (65306-41-4) → o-Nitrobenzenesulfenylprolyl-Nδ-benzyloxycarbonylornithine Benzyl Ester (88681-60-1)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 24h; Ambient temperature;

DOI:10.1135/cccc19832862

Reference yield: 93.0%

Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteine Azide (88681-62-3) + o-Nitrobenzenesulfenylprolyl-Nδ-benzyloxycarbonylornithine Benzyl Ester (88681-60-1) → Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-Nδ-benzyloxycarbonylornithine Benzyl Ester (88681-59-8)

Guidance literature:

With 1-ethyl-piperidine; In N,N-dimethyl-formamide; at 0 ℃; for 60h; Label VI used as hydrochloride;

DOI:10.1135/cccc19832862

upstream raw materials:

(S)-2-amino-5-benzyloxycarbonylamino-pentanoic acid benzyl ester hydrochloride

o-Nitrobenzenesulfenylproline 2,4,5-trichlorophenyl Ester

Downstream raw materials:

Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

Refernces