n-Methyl-4-(p-formylstyryl)pyridinium methylsulfate

Base Information

• Chemical Name: n-Methyl-4-(p-formylstyryl)pyridinium methylsulfate
• CAS No.: 74401-04-0
• Molecular Formula: C16H17NO5S
• Molecular Weight: 335.381
• European Community (EC) Number: 418-240-3,616-086-3
• Mol file: 74401-04-0.mol

Synonyms:n-methyl-4-(p-formylstyryl)pyridinium methylsulfate;74401-04-0;EC 418-240-3;4-[(E)-2-(1-methylpyridin-1-ium-4-yl)ethenyl]benzaldehyde;methyl sulfate;SCHEMBL20298611;HQMZBKRNRWIDME-SQQVDAMQSA-M;4-(4-Formylstyryl)-1-methylpyridin-1-ium methyl sulfate

Chemical Property of n-Methyl-4-(p-formylstyryl)pyridinium methylsulfate

Chemical Property:

• PSA: 95.76000
• Density: 1.28[at 20℃]
• LogP: 2.66780
• Water Solubility.: 327g/L at 20℃
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 335.08274382
• Heavy Atom Count: 23
• Complexity: 349

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 43-52/53
• Safety Statements: 22-24-37-61

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+]1=CC=C(C=C1)C=CC2=CC=C(C=C2)C=O.COS(=O)(=O)[O-]
• Isomeric SMILES: C[N+]1=CC=C(C=C1)/C=C/C2=CC=C(C=C2)C=O.COS(=O)(=O)[O-]

Technology Process of n-Methyl-4-(p-formylstyryl)pyridinium methylsulfate

There total 1 articles about n-Methyl-4-(p-formylstyryl)pyridinium methylsulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

terephthalaldehyde, (623-27-8) + 1,4-dimethyl-pyridinium; methyl sulfate (24866-73-7) → 4-[2-(4-formylphenyl)ethenyl]-1-methylpyridin-1-ium methyl sulfate (74401-04-0)

Guidance literature:

With piperidine; In methanol; for 6h; Time; Reflux;

Reference yield:

4-[2-(4-formylphenyl)ethenyl]-1-methylpyridin-1-ium methyl sulfate (74401-04-0) → C30H28N2O2(2+)

Guidance literature:

In water; UV-irradiation;

DOI:10.1016/j.carbpol.2011.05.006

Reference yield:

4-[2-(4-formylphenyl)ethenyl]-1-methylpyridin-1-ium methyl sulfate (74401-04-0) → C30H28N2O2(2+)*2CH3O4S(1-)

Guidance literature:

UV-irradiation;

DOI:10.1039/c4ra11792a

upstream raw materials:

terephthalaldehyde,

1,4-dimethyl-pyridinium; methyl sulfate

Refernces