(E)-[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate

Base Information

• Chemical Name: (E)-[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate
• CAS No.: 1221557-69-2
• Molecular Formula: C₄₂H₅₅BrN₂O₁₂
• Molecular Weight: 859.809
• Mol file: 1221557-69-2.mol

Synonyms:(E)-[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate

Chemical Property of (E)-[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate

There total 1 articles about (E)-[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C30H33BrN2O12 (1221557-64-7) + capsaicin (404-86-4,912457-62-6) → (E)-[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate (1221557-69-2)

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; Inert atmosphere; Darkness;

DOI:10.1021/jo100368w

Reference yield: 95.0%

(E)-[8-[bis(tert-butoxycarbonylmethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate (1221557-69-2) → (E)-[8-[bis(carboxymethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate (1221557-70-5)

Guidance literature:

With water; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere; Darkness;

DOI:10.1021/jo100368w

upstream raw materials:

C₃₀H₃₃BrN₂O₁₂

capsaicin

Downstream raw materials:

(E)-[8-[bis(carboxymethyl)aminomethyl]-6-bromo-7-hydroxycoumarin-4-yl]methyl 2-methoxy-4-[(8-methylnon-6-enamido)methyl]phenyl carbonate

Refernces