Technology Process of N(1)-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin
There total 7 articles about N(1)-Benzyloxycarbonyl-6,17-dihydroxy-7,10,18-trioxo-6,11,17-triazanonadecylamin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Py
2: acetic anhydride / 5 h / 95 - 100 °C
3: (i) NaOMe, MeOH, (ii) /BRN= 898057/, THF
4: (i) aq. NH4Cl, Zn, EtOH, (ii) /BRN= 385737/, Py
With
pyridine;
In
acetic anhydride;
DOI:10.1002/hlca.19620450228
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aq. NH4Cl, Zn / ethanol
2: Py
3: acetic anhydride / 5 h / 95 - 100 °C
4: (i) NaOMe, MeOH, (ii) /BRN= 898057/, THF
5: (i) aq. NH4Cl, Zn, EtOH, (ii) /BRN= 385737/, Py
With
pyridine; ammonium chloride; zinc;
In
ethanol; acetic anhydride;
DOI:10.1002/hlca.19620450228
- Guidance literature:
-
Multi-step reaction with 6 steps
1: aq. NaOH
2: aq. NH4Cl, Zn / ethanol
3: Py
4: acetic anhydride / 5 h / 95 - 100 °C
5: (i) NaOMe, MeOH, (ii) /BRN= 898057/, THF
6: (i) aq. NH4Cl, Zn, EtOH, (ii) /BRN= 385737/, Py
With
pyridine; sodium hydroxide; ammonium chloride; zinc;
In
ethanol; acetic anhydride;
DOI:10.1002/hlca.19620450228