ALLYL ISOPROPYL SULPHIDE

Base Information

• Chemical Name: ALLYL ISOPROPYL SULPHIDE
• CAS No.: 50996-72-0
• Molecular Formula: C6H12S
• Molecular Weight: 116.227
• Hs Code.: 2930909090
• Mol file: 50996-72-0.mol

Synonyms:1-Propene, 3-[(1-methylethyl)thio]-;3-(Isopropylsulfanyl)-1-propene;ALLYL ISO-PROPYL SULFIDE;ALLYL ISOPROPYL SULPHIDE

Chemical Property of ALLYL ISOPROPYL SULPHIDE

Chemical Property:

• Vapor Pressure: 10mmHg at 25°C
• Refractive Index: 1.46
• Boiling Point: 134.4°C at 760 mmHg
• Flash Point: 25.5°C
• PSA: 25.30000
• Density: 0.848g/cm³
• LogP: 2.31400

Purity/Quality:

98%Min ^*data from raw suppliers

ALLYL ISOPROPYL SULPHIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R11:Highly flammable.; R36/37/38:Irritating to eyes, respiratory system and skin.
• Hazard Codes: R11:Highly flammable.; R36/37/38:Irritating to eyes, respiratory system and skin.
• Statements: R11:Highly flammable.; R36/37/38:Irritating to eyes, respiratory system and skin.
• Safety Statements: S16:Keep away from sources of ignition - No smoking.; S26:In case of contact with eyes, rinse immediately with plenty of

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ALLYL ISOPROPYL SULPHIDE

There total 18 articles about ALLYL ISOPROPYL SULPHIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

benzoic acid 4-allyloxycarbonylbutyl ester (1333925-51-1) + 2-propanethiol (75-33-2) → 4-benzoyloxybutan-1-ol (32651-37-9) + allylisopropyl sulfide (50996-72-0) + carbon dioxide (124-38-9,18923-20-1)

Guidance literature:

With [Bu₄N][Fe(CO)3(NO)]; tris(2,4,6-trimethylphenyl)phosphine; In ethanol; at 40 ℃; Inert atmosphere;

DOI:10.1021/ol202270g

Reference yield: 100.0%

menthyl allyl carbonate (76648-56-1) + 2-propanethiol (75-33-2) → allylisopropyl sulfide (50996-72-0) + carbon dioxide (124-38-9,18923-20-1) + (-)-menthol (2216-51-5)

Guidance literature:

With Roussin's red salt ester; tetrabutylammomium bromide; potassium hydride; In tetrahydrofuran; ethanol; at 40 ℃; for 14h;

DOI:10.1021/ol202270g

Reference yield: 99.0%

dodecyl allyl carbonate (16308-67-1) + 2-propanethiol (75-33-2) → 1-dodecyl alcohol (112-53-8) + allylisopropyl sulfide (50996-72-0) + carbon dioxide (124-38-9,18923-20-1)

Guidance literature:

With Roussin's red salt ester; tetrabutylammomium bromide; potassium hydride; In tetrahydrofuran; ethanol; at 40 ℃;

DOI:10.1021/ol202270g

upstream raw materials:

carbonic acid allyl ester 4-(tetrahydropyran-2-yloxy)butyl ester

2-propanethiol

benzoic acid 4-allyloxycarbonylbutyl ester

allyl 4-(fluorenymethyloxy)butylcarbonate

Downstream raw materials:

allyldimethylphenylsilane

thioacetone

1-phenyl-4-(isopropylthio)-3-butenol

erythro-1-phenyl-2-(isopropylthio)-3-butenol

Refernces