1-p-toluidino-1-deoxy-D-glucitol

Base Information

• Chemical Name: 1-p-toluidino-1-deoxy-D-glucitol
• CAS No.: 3051-98-7
• Molecular Formula: C₁₃H₂₁NO₅
• Molecular Weight: 271.313
• Mol file: 3051-98-7.mol

Synonyms:

Chemical Property of 1-p-toluidino-1-deoxy-D-glucitol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-p-toluidino-1-deoxy-D-glucitol

There total 3 articles about 1-p-toluidino-1-deoxy-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-toluidine (106-49-0,12221-03-3) + D-Glucono-1,5-lactone (90-80-2,1335-57-5,4253-68-3) → 1-p-toluidino-1-deoxy-D-glucitol (3051-98-7,98244-19-0)

Guidance literature:

With potassium hydroxide; platinum; at 65 ℃; under 121359 Torr; Hydrogenation;

DOI:10.1021/ja01213a029

Reference yield:

D-glucose (50-99-7) + p-toluidine (106-49-0,12221-03-3) → 1-p-toluidino-1-deoxy-D-glucitol (3051-98-7,98244-19-0)

Guidance literature:

With methanol; und Hydrieren des Reaktionsprodukts in Methanol an Palladium/Kohle bei 30-50grad/25 at;

DOI:10.1002/hlca.193501801187

Reference yield:

D-Galactose (59-23-4) + p-toluidine (106-49-0,12221-03-3) → 1-p-toluidino-D-1-deoxy-galactitol (3051-98-7,98244-19-0)

Guidance literature:

With hydrogenchloride; Versetzen des Reaktionsgemisches mit Aethanol und wss.Natronlauge und anschliessend Hydrieren an Platin;

upstream raw materials:

D-glucose

p-toluidine

D-Glucono-1,5-lactone

D-Galactose