acenaphtho[1,2-c]thiophene

Base Information

• Chemical Name: acenaphtho[1,2-c]thiophene
• CAS No.: 206-20-2
• Molecular Formula: C₁₄H₈S
• Molecular Weight: 208.284
• Mol file: 206-20-2.mol

Synonyms:

Chemical Property of acenaphtho[1,2-c]thiophene

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acenaphtho[1,2-c]thiophene

There total 2 articles about acenaphtho[1,2-c]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

dimethyl thioether-α,α'-bis(triphenylphosphonium) dichloride (55304-69-3) + acenaphthene quinone (82-86-0) → acenaphtho[1,2-c]thiophene (206-20-2)

Guidance literature:

With lithium ethoxide; In ethanol; N,N-dimethyl-formamide; for 21h; Ambient temperature;

Reference yield:

thiobis(methyltriphenylphosphonium) dibromide (4973-47-1) + acenaphthene quinone (82-86-0) → acenaphtho[1,2-c]thiophene (206-20-2)

Guidance literature:

With n-butyllithium;

DOI:10.1080/10426509708545577

upstream raw materials:

dimethyl thioether-α,α'-bis(triphenylphosphonium) dichloride

acenaphthene quinone

thiobis(methyltriphenylphosphonium) dibromide

Refernces

• 1、 Lefkaditis, D. A.,Nicolaides, D. N.,Papageorgiou, G. K.,Stephanidou-Stephanatou, J.. "Synthesis of Acenaphthoheterocycles and Spiro". . p. 227 - 230. Retrieved 2007/10/02.