Benzylideneaminoisatin

Base Information Edit

Chemical Name:Benzylideneaminoisatin
CAS No.:10604-20-3
Molecular Formula:C15H10N2O2
Molecular Weight:250.257
Hs Code.:
DSSTox Substance ID:DTXSID20706633
Mol file:10604-20-3.mol

Synonyms:benzylideneaminoisatin;10604-20-3;1-(benzylideneamino)indole-2,3-dione;1-(benzylideneamino)-1H-indole-2,3-dione;DTXSID20706633;DVZBWPYYJMHVSV-UHFFFAOYSA-N

Suppliers and Price of Benzylideneaminoisatin

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Benzylideneaminoisatin Edit

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:250.074227566
Heavy Atom Count:19
Complexity:399

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=NN2C3=CC=CC=C3C(=O)C2=O

Technology Process of Benzylideneaminoisatin

There total 6 articles about Benzylideneaminoisatin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 79-37-8
oxalyl dichloride

: 588-64-7
benzaldehyde phenylhydrazone

: 10604-20-3
1-(benzylideneamino)indoline-2,3-dione

Guidance literature:: oxalyl dichloride; benzaldehyde phenylhydrazone; In dichloromethane; for 2h; Reflux;

With aluminum (III) chloride; In dichloromethane; Reflux; Cooling with ice;
DOI:10.1007/s10895-013-1229-3

Reference yield:

: 109411-83-8
oxalic acid-(benzylidene-phenyl-hydrazide)-chloride

: 10604-20-3
1-(benzylideneamino)indoline-2,3-dione

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 0 - 30 ℃; Reflux; Inert atmosphere;

Reference yield:

: 100-63-0
phenylhydrazine

: 10604-20-3
1-(benzylideneamino)indoline-2,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: water / 3 h / 25 - 30 °C / Inert atmosphere

2: dichloromethane / 3 h / -40 °C

3: aluminum (III) chloride / dichloromethane / 0 - 30 °C / Reflux; Inert atmosphere

With aluminum (III) chloride; In dichloromethane; water;