Fe(III)(NO)(TCl₂PC)

Base Information

• Chemical Name: Fe(III)(NO)(TCl₂PC)
• CAS No.: 475278-12-7
• Molecular Formula: C₃₇H₁₇Cl₆FeN₅O
• Molecular Weight: 816.14
• Mol file: 475278-12-7.mol

Synonyms:

Chemical Property of Fe(III)(NO)(TCl₂PC)

Chemical Property:

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Technology Process of Fe(III)(NO)(TCl₂PC)

There total 1 articles about Fe(III)(NO)(TCl₂PC) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.6%

Fe(5,10,15-tris(2.6-dichlorophenyl)corrole(3-))Cl (431892-19-2) + sodium nitrite (7632-00-0) → Fe(III)(NO)(TCl2PC) (475278-12-7) + Fe(III)(NO)((O2N)2TCl2PC)

Guidance literature:

In N,N-dimethyl-formamide; addn. of sodium nitrite to DMF soln. of iron compd., keeping for 45 min; addn. of water, filtration, dissolving in CH2Cl2, drying over Na2SO4, evapn., chromy. (silica gel), recrystn. (CH2Cl2/methanol (1/2));

DOI:10.1021/ic3002459

upstream raw materials:

Fe(5,10,15-tris(2.6-dichlorophenyl)corrole^(3-))Cl

sodium nitrite

Refernces