C₂₉H₃₄N₆O₁₆P₂

Base Information

• Chemical Name: C₂₉H₃₄N₆O₁₆P₂
• CAS No.: 1381944-93-9
• Molecular Formula: C₂₉H₃₄N₆O₁₆P₂
• Molecular Weight: 784.567
• Mol file: 1381944-93-9.mol

Synonyms:

Chemical Property of C₂₉H₃₄N₆O₁₆P₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₄N₆O₁₆P₂

There total 5 articles about C₂₉H₃₄N₆O₁₆P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Guanosine 5'-triphosphate (86-01-1,72490-81-4) → C29H34N6O16P2 (1381944-93-9)

Guidance literature:

Multi-step reaction with 3 steps

1: inorganic pyrophosphatase; L-fucokinase pyrophosphorylase; tris hydrochloride; manganese(ll) chloride; ATP / 12 h / 37 °C / Enzymatic reaction

2: palladium 10% on activated carbon; hydrogen / water / 0.25 h

3: N,N-dimethyl-formamide / 50 °C / pH 8.1 / aq. phosphate buffer

With inorganic pyrophosphatase; palladium 10% on activated carbon; L-fucokinase pyrophosphorylase; hydrogen; tris hydrochloride; manganese(ll) chloride; ATP; In water; N,N-dimethyl-formamide;

DOI:10.1002/adsc.201100940

Reference yield:

6-Azido-β-L-fucose (138332-00-0,138332-01-1) → C29H34N6O16P2 (1381944-93-9)

Guidance literature:

Multi-step reaction with 3 steps

1: inorganic pyrophosphatase; L-fucokinase pyrophosphorylase; tris hydrochloride; manganese(ll) chloride; ATP / 12 h / 37 °C / Enzymatic reaction

2: palladium 10% on activated carbon; hydrogen / water / 0.25 h

3: N,N-dimethyl-formamide / 50 °C / pH 8.1 / aq. phosphate buffer

With inorganic pyrophosphatase; palladium 10% on activated carbon; L-fucokinase pyrophosphorylase; hydrogen; tris hydrochloride; manganese(ll) chloride; ATP; In water; N,N-dimethyl-formamide;

DOI:10.1002/adsc.201100940

Reference yield:

6-azide-6-deoxy-β-L-galactopyranos-1-yl-guanosine 5'-diphosphate (912921-33-6) → C29H34N6O16P2 (1381944-93-9)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / water / 0.25 h

2: N,N-dimethyl-formamide / 50 °C / pH 8.1 / aq. phosphate buffer

With palladium 10% on activated carbon; hydrogen; In water; N,N-dimethyl-formamide;

DOI:10.1002/adsc.201100940

upstream raw materials:

6-azide-6-deoxy-β-L-galactopyranos-1-yl-guanosine 5'-diphosphate

guanosine 5'-diphospho-6-amino-β-L-fucopyranoside

Guanosine 5'-triphosphate

6-Azido-β-L-fucose

Refernces