2,4,5,4'-Tetramethoxy-benzil

Base Information

• Chemical Name: 2,4,5,4'-Tetramethoxy-benzil
• CAS No.: 109469-77-4
• Molecular Formula: C₁₈H₁₈O₆
• Molecular Weight: 330.337
• Mol file: 109469-77-4.mol

Synonyms:

Chemical Property of 2,4,5,4'-Tetramethoxy-benzil

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,5,4'-Tetramethoxy-benzil

There total 9 articles about 2,4,5,4'-Tetramethoxy-benzil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4',6,7-trimethoxy-isoflavone (798-61-8) → 2,4,5,4'-Tetramethoxy-benzil (109469-77-4)

Guidance literature:

Multi-step reaction with 3 steps

1: KOH / aq. ethanol

2: O₂, KOH / aq. ethanol

3: K₂CO₃

With potassium hydroxide; oxygen; potassium carbonate; In ethanol;

DOI:10.1039/jr9600001491

Reference yield:

p-methoxybenzylnitrile (104-47-2) → 2,4,5,4'-Tetramethoxy-benzil (109469-77-4)

Guidance literature:

Multi-step reaction with 3 steps

1: ZnCl₂, HCl / diethyl ether

2: O₂, KOH / aq. ethanol

3: K₂CO₃

With hydrogenchloride; potassium hydroxide; oxygen; potassium carbonate; zinc(II) chloride; In diethyl ether; ethanol;

DOI:10.1039/jr9600001491

Reference yield:

3,4-dimethoxyphenol (2033-89-8) → 2,4,5,4'-Tetramethoxy-benzil (109469-77-4)

Guidance literature:

Multi-step reaction with 3 steps

1: ZnCl₂, HCl / diethyl ether

2: O₂, KOH / aq. ethanol

3: K₂CO₃

With hydrogenchloride; potassium hydroxide; oxygen; potassium carbonate; zinc(II) chloride; In diethyl ether; ethanol;

DOI:10.1039/jr9600001491

upstream raw materials:

2,4,5-trimethoxyphenyl-4'-methoxybenzyl ketone

4',6,7-trimethoxy-isoflavone

3,4-dimethoxyphenol

methoxyhydroquinone