Technology Process of C27H24F6N2O5S
There total 11 articles about C27H24F6N2O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) iodide; dichlorobis(tri-O-tolylphosphine)palladium; triethylamine;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 2h;
DOI:10.1016/j.bmcl.2011.09.018
- Guidance literature:
-
Multi-step reaction with 8 steps
1: aluminum (III) chloride / 1,2-dichloro-ethane / 0 - 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 48 h
3: toluene-4-sulfonic acid
4: n-butyllithium / 2 h / -78 °C
5: hydrogenchloride / methanol / 20 °C
6: sodium periodate; ruthenium trichloride / acetonitrile / 5 h / 20 °C
7: aluminium; mercury dichloride / tetrahydrofuran / 20 - 40 °C
8: copper(l) iodide; dichlorobis(tri-O-tolylphosphine)palladium; triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C
With
hydrogenchloride; aluminum (III) chloride; ruthenium trichloride; sodium periodate; copper(l) iodide; lithium aluminium tetrahydride; n-butyllithium; dichlorobis(tri-O-tolylphosphine)palladium; toluene-4-sulfonic acid; triethylamine; aluminium; mercury dichloride;
In
tetrahydrofuran; methanol; 1,2-dichloro-ethane; acetonitrile;
8: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.09.018
- Guidance literature:
-
Multi-step reaction with 5 steps
1: n-butyllithium / 2 h / -78 °C
2: hydrogenchloride / methanol / 20 °C
3: sodium periodate; ruthenium trichloride / acetonitrile / 5 h / 20 °C
4: aluminium; mercury dichloride / tetrahydrofuran / 20 - 40 °C
5: copper(l) iodide; dichlorobis(tri-O-tolylphosphine)palladium; triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C
With
hydrogenchloride; ruthenium trichloride; sodium periodate; copper(l) iodide; n-butyllithium; dichlorobis(tri-O-tolylphosphine)palladium; triethylamine; aluminium; mercury dichloride;
In
tetrahydrofuran; methanol; acetonitrile;
5: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.09.018