[C₅H₄NC(CH₃)(CH₂NC₆H₂(CH₃)3)2]Zr(methyl)3[Li*diethyl ether]

Base Information

• Chemical Name: [C₅H₄NC(CH₃)(CH₂NC₆H₂(CH₃)3)2]Zr(methyl)3[Li*diethyl ether]
• CAS No.: 486413-21-2
• Molecular Formula: C₄H₁₀O*C₃₀H₄₂N₃Zr*Li
• Molecular Weight: 616.971
• Mol file: 486413-21-2.mol

Synonyms:

Chemical Property of [C₅H₄NC(CH₃)(CH₂NC₆H₂(CH₃)3)2]Zr(methyl)3[Li*diethyl ether]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [C₅H₄NC(CH₃)(CH₂NC₆H₂(CH₃)3)2]Zr(methyl)3[Li*diethyl ether]

There total 1 articles about [C₅H₄NC(CH₃)(CH₂NC₆H₂(CH₃)3)2]Zr(methyl)3[Li*diethyl ether] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

diethyl ether (60-29-7,927820-24-4) + [(C5H4N)C(CH3)(CH2N(C6H2(CH3)3))2]Zr(CH3)2 (293764-40-6) + methyllithium (917-54-4) → [C5H4NC(CH3)(CH2NC6H2(CH3)3)2]Zr(methyl)3[Li*diethyl ether] (486413-21-2)

Guidance literature:

In diethyl ether; N2; addn. of methyllithium as 4.4 M ether soln. to ether suspn. of Zr complex at -30° C, stirring at room temp. for 10 min; filtration through Celite, drying the filtrate in vac.; elem. anal.;

DOI:10.1021/om0207055

upstream raw materials:

diethyl ether

[(C₅H₄N)C(CH₃)(CH₂N(C₆H₂(CH₃)3))2]Zr(CH₃)2

methyllithium

Refernces